ORIGINAL ARTICLE
Thermal Effects on the Structural and Mechanical Microstructure Parameters of Siliceous Sandstone from Kielce Upland
 
More details
Hide details
1
Department of Geotechnics, Hydrotechnics, Underground and Hydraulic Engineering, Faculty of Civil Engineering, Wroclaw University of Science and Technology, Wrocław, Poland
 
 
Submission date: 2024-11-26
 
 
Final revision date: 2025-01-17
 
 
Acceptance date: 2025-01-26
 
 
Online publication date: 2025-02-10
 
 
Publication date: 2025-02-10
 
 
Corresponding author
Michał Patryk Pachnicz   

Department of Civil Engineering, Wroclaw University of Science and Technology, pl. Grunwaldzki 11, 50-377, Wrocław, Poland
 
 
Civil and Environmental Engineering Reports 2025;35(1):250-271
 
KEYWORDS
TOPICS
ABSTRACT
This study explores the thermal evolution of the microstructure and mechanical properties of Jurassic sandstone from the Kielce Upland, subjected to temperatures between 20°C and 1000°C. Combining microcomputed tomography (micro-CT) and nanoindentation techniques, it analyzes how geometric changes affect mechanical parameters. Key features like porosity, pore size distribution, and solid matrix thickness were assessed alongside indentation modulus (MIT) and hardness (HIT). The results reveal a strong correlation between microstructural changes and mechanical responses. At 200°C, microstructural compaction and thermal tightening lead to temporary strengthening. Above 600°C, increased porosity, microcrack formation, and rock matrix degradation cause significant reductions in mechanical properties. Reconstructed grayscale values are identified as reliable estimators for mechanical property changes, particularly for indentation modulus, when baseline parameters are available.
REFERENCES (62)
1.
Ma, X, Dong, W, Hu, D and Zhou, H 2023. Mechanical properties of granite at high temperature subjected to true triaxial compression. International Journal of Rock Mechanics and Mining Sciences 164, 105313.
 
2.
Li, Y, Zhai, Y, Xie, Y and Meng, F 2023. Research on the Impact Mechanical Properties of Real-Time High-Temperature Granite and a Coupled Thermal–Mechanical Constitutive Model. Materials 16, 2773.
 
3.
Hou, B, Sun, F, Xue, S and Zhang, X 2022. Experimental study on mechanical properties and porosity and permeability of rock in high temperature environment. Journal of Physics: Conference Series 2368, 012031.
 
4.
Dean, SW, Takarli, M and Prince-Agbodjan, W 2008. Temperature Effects on Physical Properties and Mechanical Behavior of Granite: Experimental Investigation of Material Damage. Journal of ASTM International 5, 100464.
 
5.
PG, R, Viete, DR, Chen, BJ and Perera, MSA 2012. Transformation plasticity and the effect of temperature on the mechanical behaviour of Hawkesbury sandstone at atmospheric pressure. Engineering Geology 151, 120–127.
 
6.
Sygała, A, Bukowska, M and Janoszek, T 2013. High Temperature Versus Geomechanical Parameters of Selected Rocks – The Present State of Research. Journal of Sustainable Mining 12, 45–51.
 
7.
Tian, H, Kempka, T, Yu, S and Ziegler, M 2016. Mechanical Properties of Sandstones Exposed to High Temperature. Rock Mechanics and Rock Engineering 49, 321–327.
 
8.
Yasuhara, H, Kinoshita, N, Ohfuji, H, Takahashi, M, Ito, K and Kishida, K 2015. Long‐term observation of permeability in sedimentary rocks under high‐temperature and stress conditions and its interpretation mediated by microstructural investigations. Water Resources Research 51, 5425–5449.
 
9.
Lintao, Y, Marshall, AM, Wanatowski, D, Stace, R and Ekneligoda, T 2017. Effect of high temperatures on sandstone – a computed tomography scan study. International Journal of Physical Modelling in Geotechnics 17, 75–90.
 
10.
Lei, R, Wang, Y, Zhang, L, Liu, B, Long, K, Luo, P and Wang, Y 2019. The evolution of sandstone microstructure and mechanical properties with thermal damage. Energy Science & Engineering 7, 3058–3075.
 
11.
Cheng, C and Milsch, H 2020. Permeability Variations in Illite‐Bearing Sandstone: Effects of Temperature and NaCl Fluid Salinity. Journal of Geophysical Research: Solid Earth 125.
 
12.
Zheng, Y, Zhang, L, Wu, P, Guo, X, Li, M and Zhu, F 2024. Physical and Mechanical Properties and Damage Mechanism of Sandstone at High Temperatures. Applied Sciences 2024.
 
13.
Fan, LF, Gao, JW, Wu, ZJ, Yang, SQ and Ma, GW 2018. An investigation of thermal effects on micro-properties of granite by X-ray CT technique. Applied Thermal Engineering 140, 505–519.
 
14.
Shen, Y-J, Zhang, Y-L, Gao, F, Yang, G-S and Lai, X-P 2018. Influence of Temperature on the Microstructure Deterioration of Sandstone. Energies 11, 1753.
 
15.
Li, J, Du, Z-W and Guo, Z-P 2020. Effect of High Temperature (600°C) on Mechanical Properties, Mineral Composition, and Microfracture Characteristics of Sandstone. Advances in Materials Science and Engineering 2020.
 
16.
Różański, A, Różańska, A, Sobótka, M, Pachnicz, M and Bukowska, M 2021. Identification of changes in mechanical properties of sandstone subjected to high temperature: meso-and micro-scale testing and analysis. Archives of Civil and Mechanical Engineering 21, 28.
 
17.
Elliott, JC and Dover, SD 1982. X‐ray microtomography. Journal of Microscopy 126, 211–213.
 
18.
Stock, SR 1999. X-ray microtomography of materials. International Materials Reviews 44, 141–164.
 
19.
Maire, E, Buffière, JY, Salvo, L, Blandin, JJ, Ludwig, W and Létang, JM 2001. On the Application of X-ray Microtomography in the Field of Materials Science. Advanced Engineering Materials B, 539.
 
20.
Stock, SR 2008. Recent advances in X-ray microtomography applied to materials. International Materials Reviews 53, 129–181.
 
21.
Landis, EN and Keane, DT 2010. X-ray microtomography. Materials characterization 61, 1305–1316.
 
22.
Fischer-Cripps, AC and Nicholson, DW 2004. Nanoindentation. Mechanical engineering series. Appl. Mech. Rev 57, B12–B12.
 
23.
Schuh, CA 2006. Nanoindentation studies of materials. Materials today 9, 32–40.
 
24.
Mukhopadhyay, NK and Paufler, P 2006. Micro- and nanoindentation techniques for mechanical characterisation of materials. International Materials Reviews 51, 209–245.
 
25.
Oyen, ML and Cook, RF 2009. A practical guide for analysis of nanoindentation data. Journal of the mechanical behavior of biomedical materials 2, 396–407.
 
26.
Lucca, DA, Herrmann, K and Klopfstein, MJ 2010. Nanoindentation: Measuring methods and applications. CIRP annals 59, 803–819.
 
27.
Appoloni, CR, Fernandes, CP and Rodrigues, CRO 2007. X-ray microtomography study of a sandstone reservoir rock. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment 580, 629–632.
 
28.
Zhu, W, Hughes, JJ, Bicanic, N and Pearce, CJ 2007. Nanoindentation mapping of mechanical properties of cement paste and natural rocks. Materials characterization 58, 1189–1198.
 
29.
Zandomeneghi, D, Voltolini, M, Mancini, L, Brun, F, Dreossi, D and Polacci, M 2010. Quantitative analysis of X-ray microtomography images of geomaterials: Application to volcanic rocks. Geosphere 6, 793–804.
 
30.
Baker, DR, Mancini, L, Polacci, M, Higgins, MD, Gualda, GAR, Hill, RJ and Rivers, ML 2012. An introduction to the application of X-ray microtomography to the three-dimensional study of igneous rocks. Lithos 148, 262–276.
 
31.
Bielecki, J, Jarzyna, J, Bożek, S, Lekki, J, Stachura, Z and Kwiatek, WM 2013. Computed microtomography and numerical study of porous rock samples. Radiation Physics and Chemistry 93, 59–66.
 
32.
Shukla, P, Taneja, S, Sondergeld, C and Rai, C 2015. Nanoindentation Measurements on Rocks. Fracture, Fatigue, Failure, and Damage Evolution, Volume 5. J. Carroll and S. Daly, eds. Springer International Publishing, 99–105.
 
33.
Ma, Z, Pathegama Gamage, R and Zhang, C 2020. Application of nanoindentation technology in rocks: a review. Geomechanics and Geophysics for Geo-Energy and Geo-Resources 6, 60.
 
34.
Górska-Zabielska, M 2021. The Rock Garden of the Institute of Geography and Environmental Sciences, Jan Kochanowski University—A New Geo-Site in Kielce, Central Poland. Geosciences 11.
 
35.
Folk, RL 1954. The Distinction between Grain Size and Mineral Composition in Sedimentary-Rock Nomenclature. The Journal of Geology 62, 344–359.
 
36.
Lambert, JH 1760. I. H. Lambert ... Photometria sive de mensura et gradibus luminis, colorum et umbrae [Photometry or the measurement and degrees of light, colors and shade]. Augustae Vindelicorum : sumptibus viduae Eberhardi Klett typis Chistophori Petri Detleffsen.
 
37.
Beer 1852. Bestimmung der Absorption des rothen Lichts in farbigen Flüssigkeiten [Determination of the absorption of red light in colored liquids]. Annalen der Physik. 162, 78–88.
 
38.
Ingle, DJ 1988. Crouch. SR Spectrochemical Analysis Prentice Hall.
 
39.
Otsu, N 1979. A Threshold Selection Method from Gray-Level Histograms. IEEE Transactions on Systems, Man, and Cybernetics 9, 62–66.
 
40.
Bruker-MicroCT CT-Analyser: morphometric parameters in 3D and 2D. Bruker.
 
41.
Constantinides, G, Chandran, K.R, Ulm, F.-J and Van Vliet, K.J 2006. Grid indentation analysis of composite microstructure and mechanics: Principles and validation. Materials Science and Engineering: A 430, 189–202.
 
42.
Hoan, PT and Thuong, NT 2021. Microstructural characteristics of ultra-high performance concrete by grid nanoindentation and statistical analysis. Journal of Science and Technology in Civil Engineering (STCE) - NUCE 15, 90–101.
 
43.
Anton Paar 2023. Quick matrix mode for grid indentation method. Anton Paar.
 
44.
Doerner, MF and Nix, WD 1986. A method for interpreting the data from depth-sensing indentation instruments. Journal of Materials Research 1, 601–609.
 
45.
Oliver, WC and Pharr, GM 2004. Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology. Journal of materials research 19, 3–20.
 
46.
Oliver, WC and Pharr, GM 1992. An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. Journal of Materials Research 7, 1564–1583.
 
47.
Velez, K, Maximilien, S, Damidot, D, Fantozzi, G and Sorrentino, F 2001. Determination by nanoindentation of elastic modulus and hardness of pure constituents of Portland cement clinker. Cement and Concrete Research 31, 555–561.
 
48.
Wang, H, Lin, H, Cao, P 2017. Correlation of UCS Rating with Schmidt Hammer Surface Hardness for Rock Mass Classification. Rock Mech Rock Eng 50, 195–203.
 
49.
Chau, KT, Wong RHC 1996. Uniaxial compressive strength and point load strength of rocks. International Journal of Rock Mechanics and Mining Sciences & Geomechanics Abstracts 33, 183–188.
 
50.
Dinçer, İ, Acar, A, Çobanoğlu, I, et al 2004. Correlation between Schmidt hardness, uniaxial compressive strength and Young’s modulus for andesites, basalts and tuffs. Bulletin of Engineering Geology and the Environment 63, 141–148.
 
51.
Basu, A, Mishra, D, Roychowdhury, K 2013. Rock failure modes under uniaxial compression, Brazilian, and point load tests. Bulletin of Engineering Geology and the Environment 72.
 
52.
Cala, M, Cyran, K, Kawa, M, Kolano, M, Lydzba, D, Pachnicz, M, Rajczakowska, M, Rózanski, A, Sobótka, M, Stefaniuk, D, Stopkowicz, A and Walach, D 2017. Identification of Microstructural Properties of Shale by combined Use of X-Ray Micro-CT and Nanoindentation Tests. ISRM European Rock Mechanics Symposium - EUROCK 2017, Ostrava, Czech Republic, June 2017.
 
53.
Gorzelańczyk, T, Pachnicz, M, Różański, A and Schabowicz, K 2019. Multi-Scale Structural Assessment of Cellulose Fibres Cement Boards Subjected to High Temperature Treatment. Materials 12, 2449.
 
54.
Gorzelańczyk, T, Pachnicz, M, Różański, A and Schabowicz, K 2020. Identification of microstructural anisotropy of cellulose cement boards by means of nanoindentation. Construction and Building Materials 257, 119515.
 
55.
Wolfram Research,Inc Mathematica, Version 12.0.
 
56.
Van Rossum, G and Drake Jr, FL 1995. Python reference manual. Centrum voor Wiskunde en Informatica Amsterdam.
 
57.
Pedregosa, F et al. 2011. Scikit-learn: Machine Learning in Python. Journal of Machine Learning Research. 12, 2825–2830.
 
58.
Eidelman, A 2020. Python Data Science Handbook by Jake VANDERPLAS (2016). Statistique et Société. 8, 45–47.
 
59.
Li, M and Liu, X 2022. Effect of Thermal Treatment on the Physical and Mechanical Properties of Sandstone: Insights from Experiments and Simulations. Rock Mechanics and Rock Engineering 55, 3171–3194.
 
60.
Schwarz, G 1978. Estimating the dimension of a model. The annals of statistics, 461–464.
 
61.
Akaike, H 1998. Information theory and an extension of the maximum likelihood principle. Selected papers of Hirotugu Akaike. 199–213.
 
62.
He, C, Mishra, B, Shi, Q, Zhao, Y, Lin, D and Wang, X 2023. Correlations between mineral composition and mechanical properties of granite using digital image processing and discrete element method. International Journal of Mining Science and Technology 33, 949–962.
 
eISSN:2450-8594
ISSN:2080-5187
Journals System - logo
Scroll to top